|
|||||||||||||
|
|||||||||||||
A Beamline for High-Pressure Studies at the Advanced Light Source with a Superconducting Bending Magnet as the Source Martin Kunz Alastair A. MacDowell Wendel A. Caldwell Daniella Cambie Richard S. Celestre Edward E. Domning Robert M. Duarte Arianna E. Gleason James M. Glossinger Nicholas Kelez David W. Plate Tony Yu Joeseph M. Zaug Howard A. Padmore Raymond Jeanloz A. Paul Alivisatos Simon M. Clark
ABSTRACT: A new facility for high-pressure diffraction and spectroscopy using diamond anvil
high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline
benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet
(superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred
from the superbend to the experimental enclosure by the brightness preserving optics of the
beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a
Kohzu monochromator vessel with a Si(111) crystals (E/DE ~; 7000) and a W/B4C multilayers (E/DE ~;
100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental
enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample
positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim
at the installation of a second end station dedicated for in situ laser-heating on one hand and a
dedicated high-pressure single-crystal station, applying both monochromatic as well as
polychromatic techniques.
SUGGESTED CITATION:
| |||||||||||||
|
|||||||||||||