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Lawrence Berkeley National Laboratory
University of California

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A Beamline for High-Pressure Studies at the Advanced Light Source with a Superconducting Bending Magnet as the Source
Martin Kunz
Alastair A. MacDowell
Wendel A. Caldwell
Daniella Cambie
Richard S. Celestre
Edward E. Domning
Robert M. Duarte
Arianna E. Gleason
James M. Glossinger
Nicholas Kelez
David W. Plate
Tony Yu
Joeseph M. Zaug
Howard A. Padmore
Raymond Jeanloz
A. Paul Alivisatos
Simon M. Clark

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ABSTRACT:

A new facility for high-pressure diffraction and spectroscopy using diamond anvil high-pressure cells has been built at the Advanced Light Source on Beamline 12.2.2. This beamline benefits from the hard X-radiation generated by a 6 Tesla superconducting bending magnet (superbend). Useful x-ray flux is available between 5 keV and 35 keV. The radiation is transferred from the superbend to the experimental enclosure by the brightness preserving optics of the beamline. These optics are comprised of: a plane parabola collimating mirror (M1), followed by a Kohzu monochromator vessel with a Si(111) crystals (E/DE ~; 7000) and a W/B4C multilayers (E/DE ~; 100), and then a toroidal focusing mirror (M2) with variable focusing distance. The experimental enclosure contains an automated beam positioning system, a set of slits, ion chambers, the sample positioning goniometry and area detectors (CCD or image-plate detector). Future developments aim at the installation of a second end station dedicated for in situ laser-heating on one hand and a dedicated high-pressure single-crystal station, applying both monochromatic as well as polychromatic techniques.

SUGGESTED CITATION:
Martin Kunz, Alastair A. MacDowell, Wendel A. Caldwell, Daniella Cambie, Richard S. Celestre, Edward E. Domning, Robert M. Duarte, Arianna E. Gleason, James M. Glossinger, Nicholas Kelez, David W. Plate, Tony Yu, Joeseph M. Zaug, Howard A. Padmore, Raymond Jeanloz, A. Paul Alivisatos, and Simon M. Clark, "A Beamline for High-Pressure Studies at the Advanced Light Source with a Superconducting Bending Magnet as the Source" (June 30, 2005). Lawrence Berkeley National Laboratory. Paper LBNL-57453.
http://repositories.cdlib.org/lbnl/LBNL-57453

 
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